Titrimetric method determination of the content of the mass part of siliciumin feed additives
Abstract
O. V. Moravska*, T. R. Levytskyy and S. O. Vovk
The results of the development of the method for determining the mass fraction of silicium in powder samples of feed additives by the titrimetric method are presented in the article. The implementation and validation of the method was carried out with the use of feed additive of mixed type "Mikasil" produced by LLC «Globus», Ukraine. The procedure was reproduced ten times with the determination of the mass fraction of siliciumin two parallel samples. The method is based on the precipitation of silicic acid in the form of silicium-fluoride of potassium, followed by hydrolysis with hot water in the presence of chlorous calcium. The isolated hydro-chloric acid in an amount equivalent to the content of hydro-fluoric acid is titrating with alkali solution in the presence of an indicator. The results of the studies showed that the specified method for determining the mass fraction of silicium meets the standards of accuracy control for this method, namely the standard quadratic deviation (σ) is 0.52, when norm up to 0.7, when determined in two parallel samples. The results obtained indicate that the titrimetric method for determining the mass fraction of silicium in powder samples of feed additives is accurate, reliable, reproducible and economically available.